Product Notes
- 7857993 reads
From 490 to 536 g. of ethyl chloroacetate (b.p. 144–145°) is recovered by the distillation.
Although this product cannot be purified by distillation, it contains almost the theoretical amount of nitrogen as shown by Kjeldahl analysis.
During the first few hours the distillate contains ethyl acetate; the distillate obtained during the first hour, amounting to 137 ml., distils below 99° and on saturation with sodium chloride yields 115 ml. of crude ethyl acetate.
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